What products are involved?
SRV - Inline Viscosity Meter and SRD - Inline Density and Viscosity meter
What is the purpose of this article?
Compare the advantages of an in-tank or vessel and recirculation line installation for a mixing process.


1. Mixing processes

The Rheonics Type-SR sensors are used to monitor inline density and viscosity of a fluid and enable real-time control of a process. Mixing processes are a good use-case for the sensors to track changes in the properties of the fluid, for example, as solvents are added, mixing is activated, temperature is varied and as time elapses and blending or reaction progresses.

This article will focus on mixing processes that happen in tanks or vessels. Mixing tanks may be designed with inner shafts and can have recirculation lines to, among other reasons, ensure proper mixing of the fluid. 

Rheonics sensors can be ordered with different connections (visit SRV and SRD articles) to be compatible with installation in tanks and pipelines. Rheonics accessories can be used as well for mounting flexibility. 

Deciding whether to install the SR- sensor in the tank or the recirculation line, and whether to measure the viscosity or/and density changes in a mixing fluid, will come down to details of each process. For example, mixing shafts inside the tank may leave no space for sensor installations in the wall, then installation in the line is a potential solution. On the other hand, recirculation lines may not be on during the complete mixing process so cannot provide monitoring over the complete mixing process. In the next section, an analysis of each installation position is given.

Note: Each fluid will have specific characteristics and behaviors, visit this article for general recommendations for specific fluid types: Installation guidelines for different types of fluids. Processes are unique as well and often need a review of the operational, installation and targets. If needed, contact Rheonics support team for installation review of your application.


2. Comparing viscometer and density meter installation options/positions for mixing processes

Next image represents the versatility of installations from Rheonics sensors with some examples:

Figure 1: Tank and recirculation line installation examples


Table 1: Installation examples with sensor codes

Zoom-in viewSensor code
1. Long insertion from the top

SRD-X5-A370-BA20A

Connection: Flange ANSI 2” 150lb RF

2. Flush installationSRV-X4-15T

Connection: 1.5” Tri-Clamp

3. Long Tri-Clamp insertion on wall

SRV-X5-A200-B20T

Connection: 2” Tri-Clamp

4. Threaded installation on wall

SRD-X1-34N

Connection: NPT 3/4”

Recommended accessory: WOL-34NL

5. Long installation from bottom


SRD-X5-A150-BH50

Connection: DIN11851 DN50

6. Threaded installation in pipe

SRD-X1-12G

Connection: G 1/2” 

Recommended accessory: HAW-12G

7. Long insertion threaded installation in pipe elbow

SRV-A130-B1N25

Connection: NPT 1.25”

Installation in tank - process viscometer and density meter

The Rheonics SRV and SRD sensors can be installed in tank for mixing processes if:

  • Shafts or rotating blades do NOT hit the sensor probe.

  • Shafts or rotating blades do NOT interfere with the sensing elements of the probes. 

  • The sensor can be installed below the minimum fluid level in tank. This way, the sensing element of the probe will be always immersed in fluid. 

Advantages of installation in tanks are:

  • Track the complete mixing process: It is possible to track the complete process from start to finish and to trace important events (such as the addition of solvents, temperature changes, start and stop of pumps and mixers) and see how these affect the viscosity or/and density of the fluid. 

  • Versatility of installation: From the top, side wall, bottom of the tank, all installation points can be used for the Type-SR sensors. Installation of long insertion sensors have the advantage to avoid buildups or deposits around the sensing element by protuding the sensor further in the fluid.

Important consideration when installing in tank:

  • Variable flow conditions: Fluid across the sensor is likely to not have a well defined flow behavior. Rheonics sensors don’t require a specific flow rate for good readings, but constant flow rates favor stable readings. Consider that for non-Newtonian fluids, viscosity will change with flow rate due to change in apparent shear on the fluid. 

  • Higher noise: This is a possible issue with installations in tank, at least until the mixture is homogenous. However, the noise can be used as an indicator of homogeneity of the mixing. 

  • More data processing: Installation in tank may need a deeper analysis from the user to get the baseline values and filters may be needed to reduce noise and track homogeneity. The RCP software of the sensor is a useful tool for data analysis and Rheonics sensors have multiple levels of filters available to monitor and output baseline values as well as short term variations. Contact Rheonics support to learn how onboard filters can be useful for your data captures.

  • Generally, the SRD is not recommended for mixing tanks due to the variable flow that affects the readings stability. Installation in recirculation line is preferred since the probe is exposed to a controlled flow.

Installation in recirculation line - process viscometer and density meter 

The Rheonics SRV and SRD sensors can be installed in the recirculation or distribution lines if:

  • Fluid is always recirculating in line during the mixing process. Idea is to avoid oscillation between an empty and full pipe.

  • We recommend to have the fluid in motion and at nearly constant flow velocity to ensure stable, repeatable and reproducible measurements in particular when the fluid is non-Newtonian. Moving fluid ensures that there is good transfer of the fluid over the sensor and it is measuring a representative sample of the tank. Constant flow rate ensures similar shear rate for non-Newtonian fluids, ensuring apparent viscosity is measured at similar shears between samples. 

Advantages of installations in recirculation lines are:

  • Uniform flow conditions around the sensing element, which lead to constant and clean readings for viscosity.

  • Lower noise: This is a result of ensuring similar flow-induced shear rate for non-Newtonian fluids.

  • End-product detection: It is easier to ensure similarity of operating conditions (flow rate, temperature) in recirculation lines which means batch to batch comparison is done in similar conditions.


3. Further analysis of installation examples

Two main criterias should be met for the installation of the SRV and SRD sensors:

i. Immersed the sensing element completely in the fluid.

ii. Avoid stagnation or deposits around the sensing element.

Rheonics SR sensors allow multiple installation options as shown in Figure 1. Let’s review each installation example closely.


Table 2: Installation examples further considerations

InstallationConsiderations
1. Long insertion from the top
  • Good solution if installation on walls or bottom is not possible, but sensing element (see next image) should be immersed in the fluid.
  • For open tanks, consider the TMA-34N Tank mount adapter from Rheonics as alternative solution.
  • For the SRD: Full submersion ensures thermal balance along the resonator and avoid deviations on density.
2. Flush installation
  • Consider a welded flush flange for installation.
  • All dead zones should be avoided.
  • EHEDG and 3-A compatible
  • For SRD: Density deviation may happen if there is a mismatch of ambient and fluid temperature.
3. Long Tri-Clamp insertion on wall
  • Avoids stagnation zones or deposits on tank wall.
  • Useful for thick or jacketed walls.
  • Note: Ensure the sensing element is not in contact with any moving parts.
4. Threaded installation on wall
  • Standard version of the sensor. 
  • Care should be taken during installation planning to ensure there are no dead zones around the sensing element. 

5. Long installation from bottom

  • Short and flush sensor installations also possible.
6. Threaded installation in pipe
  • Rheonics offers NPT 3/4” and G1/2” threaded connections for short the sensor probe variant.
  • Installation can be done with Rheonics weldolets
  • For the SRV, perpendicular installation can be easily achieved with pipes from 2.5” up. For 1.5” and 2” pipes use Rheonics accessories. Special option for 1” is also available. 
  • For the SRD, perpendicular installation can be easily achieved with pipes from 2.5” up. Options for 2” pipes are available. Smaller sizes would require parallel installation with Rheonics flow cells.
  • For the SRD, installation with short sensors is recommended for ambient tempature applications only.
7. Long insertion threaded installation in pipe elbow
  • Protudes the sensing element in the pipe, placing the tip axially to the fluid and good flow.
  • Ideal scenario for fluids with high viscosity.
  • For the SRD, this solution with long insertion probe installed parallel to flow is useful to mantain thermal equilibrium along the resonator and use in HT (high temperature) conditions.


4. Conclusions

Both installation options, in tank or recirculation line, are valid and decision should be made based on the characteristics of the process and fluid. 

It can be said that measurements directly in mixing vessel are much more valuable in long term but need more work from the process engineering on the costumer side. Installation itself requires more effort than in the recirculation line. Sensor needs a location where the best transfer of fluid can be offered, while trying to have uniform flow characteristics. Avoiding stagnation zones would be important in both cases.